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Process for the preparation of bistriphenylsilyl chromate

Patent Number: US5698723
Date of Patent: 1997-12-16
Inventor(s): Dai Longxiu(CN); Duan Qiwei(CN); Ji Hongbo(CN); Wang Xiaoyuan(CN); Mo Jinqiang(CN); Wang Jinfeng(CN); Liu Hongmei(CN); Li Xiuqin(CN); Chen Jiuhua(CN); Gao Ping(CN)
Applicant(s): CHINA PAETO CHEMICAL CORP (CN); RESEARCH INSTITUTE OF PETROLEUM PROCESSING, SINOPEC(CN)
Application Number: 698874 19960816
Priority Number(s): CN95109750 19950817
IPC Classification: C07F11/00 ; C07F7/02
EC Classification: C07F11/00B, C07F7/08D2
U.S. Classification: 556/10;556/12;556/57;502/158
Equivalents: CN95109750


Abstract
Disclosed is a process for the preparation of bistriphenylsilyl chromate, wherein triphenylchlorosilane, potassium dichromate and any one selected from alkali metal oxides, alkali hydroxides and alkali metal carbonates are reacted in, as solvent, a mixture of glacial acetic acid and a hydrocarbon solvent at a certain temperature, whereby bistriphenylsilyl chromate having high purity can be obtained with high yield.

 

 

Research Institute of Petroleum Processing, SINOPEC
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